FIT OF THE ASSAY DATA BY GLS WITH POWER VARIANCE, THETA UNKNOWN AND ESTIMATED BY IDENTITY OLS estimate 482.553 6222.278 2.195828 1.155375 Estimate of assumed constant SD of y 100.7284 Iteration 1 Estimate of theta 0.3872 Iteration 1 GLS estimate of beta 574.9707 6196.145 2.169468 1.20847 Iteration 2 Estimate of theta 0.6567 Iteration 2 GLS estimate of beta 605.4155 6183.625 2.163816 1.231912 Iteration 3 Estimate of theta 0.726 Iteration 3 GLS estimate of beta 610.3704 6181.482 2.163051 1.236117 Iteration 4 Estimate of theta 0.7356 Iteration 4 GLS estimate of beta 610.9831 6181.234 2.162947 1.236638 Iteration 5 Estimate of theta 0.7367 Iteration 5 GLS estimate of beta 611.0536 6181.206 2.162935 1.236698 Iteration 6 Estimate of theta 0.7368 Iteration 6 GLS estimate of beta 611.0617 6181.203 2.162934 1.236705 Iteration 7 Estimate of theta 0.7368 Iteration 7 GLS estimate of beta 611.0627 6181.203 2.162933 1.236706 Iteration 8 Estimate of theta 0.7368 Iteration 8 GLS estimate of beta 611.0628 6181.203 2.162933 1.236706 Iteration 9 Estimate of theta 0.7368 Iteration 9 GLS estimate of beta 611.0628 6181.203 2.162933 1.236706 Iteration 10 Estimate of theta 0.7368 Iteration 10 GLS estimate of beta 611.0628 6181.203 2.162933 1.236706 Iteration 11 Estimate of theta 0.7368 Iteration 11 GLS estimate of beta 611.0628 6181.203 2.162933 1.236706 Iteration 12 Estimate of theta 0.7368 Iteration 12 GLS estimate of beta 611.0628 6181.203 2.162933 1.236706 Iteration 13 Estimate of theta 0.7368 Iteration 13 GLS estimate of beta 611.0628 6181.203 2.162933 1.236706 Iteration 14 Estimate of theta 0.7368 Iteration 14 GLS estimate of beta 611.0628 6181.203 2.162933 1.236706 Iteration 15 Estimate of theta 0.7368 Iteration 15 GLS estimate of beta 611.0628 6181.203 2.162933 1.236706 Iteration 16 Estimate of theta 0.7368 Iteration 16 GLS estimate of beta 611.0628 6181.203 2.162933 1.236706 Iteration 17 Estimate of theta 0.7368 Iteration 17 GLS estimate of beta 611.0628 6181.203 2.162933 1.236706 Iteration 18 Estimate of theta 0.7368 Iteration 18 GLS estimate of beta 611.0628 6181.203 2.162933 1.236706 Iteration 19 Estimate of theta 0.7368 Iteration 19 GLS estimate of beta 611.0628 6181.203 2.162933 1.236706 Iteration 20 Estimate of theta 0.7368 Iteration 20 GLS estimate of beta 611.0628 6181.203 2.162933 1.236706 Final estimate of sigma 0.242128 Final estimate of theta 0.736818 Formula: ywt ~ weightfunc(x, b1, b2, b3, b4, wt) Parameters: Estimate Std. Error t value Pr(>|t|) b1 6.111e+02 4.566e+01 13.38 1.17e-14 *** b2 6.181e+03 5.412e+01 114.22 < 2e-16 *** b3 2.163e+00 2.815e-02 76.83 < 2e-16 *** b4 1.237e+00 4.241e-02 29.16 < 2e-16 *** --- Signif. codes: 0 ‘***’ 0.001 ‘**’ 0.01 ‘*’ 0.05 ‘.’ 0.1 ‘ ’ 1 Residual standard error: 0.2421 on 32 degrees of freedom Number of iterations to convergence: 6 Achieved convergence tolerance: 5.45e-06