FIT OF THE DISSOLUTION DATA BY GLS WITH POWER VARIANCE, THETA UNKNOWN AND ESTIMATED BY IDENTITY OLS estimate 51.14444 32.4096 0.877612 1.3788 14.00983 13.60494 Estimate of assumed constant SD of y 1.897993 Iteration 1 Estimate of theta 0.9731 Iteration 1 GLS estimate of beta 50.65366 32.20246 0.899094 1.382706 13.70071 13.70648 Iteration 2 Estimate of theta 1.0572 Iteration 2 GLS estimate of beta 50.56565 32.15637 0.902053 1.384659 13.63562 13.72987 Iteration 3 Estimate of theta 1.0521 Iteration 3 GLS estimate of beta 50.57019 32.15783 0.90196 1.384608 13.63858 13.72914 Iteration 4 Estimate of theta 1.0522 Iteration 4 GLS estimate of beta 50.5701 32.15781 0.901961 1.384609 13.63853 13.72915 Iteration 5 Estimate of theta 1.0522 Iteration 5 GLS estimate of beta 50.5701 32.15781 0.901961 1.384609 13.63853 13.72915 Iteration 6 Estimate of theta 1.0522 Iteration 6 GLS estimate of beta 50.5701 32.15781 0.901961 1.384609 13.63853 13.72915 Iteration 7 Estimate of theta 1.0522 Iteration 7 GLS estimate of beta 50.5701 32.15781 0.901961 1.384609 13.63853 13.72915 Iteration 8 Estimate of theta 1.0522 Iteration 8 GLS estimate of beta 50.5701 32.15781 0.901961 1.384609 13.63853 13.72915 Iteration 9 Estimate of theta 1.0522 Iteration 9 GLS estimate of beta 50.5701 32.15781 0.901961 1.384609 13.63853 13.72915 Iteration 10 Estimate of theta 1.0522 Iteration 10 GLS estimate of beta 50.5701 32.15781 0.901961 1.384609 13.63853 13.72915 Iteration 11 Estimate of theta 1.0522 Iteration 11 GLS estimate of beta 50.5701 32.15781 0.901961 1.384609 13.63853 13.72915 Iteration 12 Estimate of theta 1.0522 Iteration 12 GLS estimate of beta 50.5701 32.15781 0.901961 1.384609 13.63853 13.72915 Iteration 13 Estimate of theta 1.0522 Iteration 13 GLS estimate of beta 50.5701 32.15781 0.901961 1.384609 13.63853 13.72915 Iteration 14 Estimate of theta 1.0522 Iteration 14 GLS estimate of beta 50.5701 32.15781 0.901961 1.384609 13.63853 13.72915 Iteration 15 Estimate of theta 1.0522 Iteration 15 GLS estimate of beta 50.5701 32.15781 0.901961 1.384609 13.63853 13.72915 Iteration 16 Estimate of theta 1.0522 Iteration 16 GLS estimate of beta 50.5701 32.15781 0.901961 1.384609 13.63853 13.72915 Iteration 17 Estimate of theta 1.0522 Iteration 17 GLS estimate of beta 50.5701 32.15781 0.901961 1.384609 13.63853 13.72915 Iteration 18 Estimate of theta 1.0522 Iteration 18 GLS estimate of beta 50.5701 32.15781 0.901961 1.384609 13.63853 13.72915 Iteration 19 Estimate of theta 1.0522 Iteration 19 GLS estimate of beta 50.5701 32.15781 0.901961 1.384609 13.63853 13.72915 Iteration 20 Estimate of theta 1.0522 Iteration 20 GLS estimate of beta 50.5701 32.15781 0.901961 1.384609 13.63853 13.72915 Final estimate of sigma 0.036305 Final estimate of theta 1.052227 Formula: ywt ~ weightfunc(x, W0, W1, beta0, beta1, tau0, tau1, v, wt) Parameters: Estimate Std. Error t value Pr(>|t|) W0 50.57010 1.44647 34.961 < 2e-16 *** W1 32.15781 1.83504 17.524 7.26e-12 *** beta0 0.90196 0.02501 36.066 < 2e-16 *** beta1 1.38461 0.33726 4.105 0.000827 *** tau0 13.63853 0.82246 16.583 1.68e-11 *** tau1 13.72915 1.87506 7.322 1.72e-06 *** --- Signif. codes: 0 ‘***’ 0.001 ‘**’ 0.01 ‘*’ 0.05 ‘.’ 0.1 ‘ ’ 1 Residual standard error: 0.0363 on 16 degrees of freedom Number of iterations to convergence: 5 Achieved convergence tolerance: 2.882e-06