FIT OF THE DISSOLUTION DATA BY GLS WITH POWER VARIANCE, THETA UNKNOWN AND ESTIMATED BY PL OLS estimate 51.14444 32.4096 0.877612 1.3788 14.00983 13.60494 Estimate of assumed constant SD of y 1.897993 Iteration 1 Estimate of theta 0.9917 Iteration 1 GLS estimate of beta 50.63708 32.19458 0.899618 1.383012 13.68883 13.71047 Iteration 2 Estimate of theta 1.1202 Iteration 2 GLS estimate of beta 50.4993 32.12456 0.904004 1.385992 13.58759 13.74600 Iteration 3 Estimate of theta 1.1353 Iteration 3 GLS estimate of beta 50.48184 32.11491 0.904576 1.386417 13.57432 13.75092 Iteration 4 Estimate of theta 1.1372 Iteration 4 GLS estimate of beta 50.4797 32.11371 0.904647 1.38647 13.57269 13.75153 Iteration 5 Estimate of theta 1.1374 Iteration 5 GLS estimate of beta 50.47944 32.11356 0.904655 1.386476 13.57249 13.75160 Iteration 6 Estimate of theta 1.1374 Iteration 6 GLS estimate of beta 50.47941 32.11354 0.904656 1.386477 13.57246 13.75161 Iteration 7 Estimate of theta 1.1374 Iteration 7 GLS estimate of beta 50.4794 32.11354 0.904656 1.386477 13.57246 13.75161 Iteration 8 Estimate of theta 1.1374 Iteration 8 GLS estimate of beta 50.4794 32.11354 0.904656 1.386477 13.57246 13.75161 Iteration 9 Estimate of theta 1.1374 Iteration 9 GLS estimate of beta 50.4794 32.11354 0.904656 1.386477 13.57246 13.75161 Iteration 10 Estimate of theta 1.1374 Iteration 10 GLS estimate of beta 50.4794 32.11354 0.904656 1.386477 13.57246 13.75161 Iteration 11 Estimate of theta 1.1374 Iteration 11 GLS estimate of beta 50.4794 32.11354 0.904656 1.386477 13.57246 13.75161 Iteration 12 Estimate of theta 1.1374 Iteration 12 GLS estimate of beta 50.4794 32.11354 0.904656 1.386477 13.57246 13.75161 Iteration 13 Estimate of theta 1.1374 Iteration 13 GLS estimate of beta 50.4794 32.11354 0.904656 1.386477 13.57246 13.75161 Iteration 14 Estimate of theta 1.1374 Iteration 14 GLS estimate of beta 50.4794 32.11354 0.904656 1.386477 13.57246 13.75161 Iteration 15 Estimate of theta 1.1374 Iteration 15 GLS estimate of beta 50.4794 32.11354 0.904656 1.386477 13.57246 13.75161 Iteration 16 Estimate of theta 1.1374 Iteration 16 GLS estimate of beta 50.4794 32.11354 0.904656 1.386477 13.57246 13.75161 Iteration 17 Estimate of theta 1.1374 Iteration 17 GLS estimate of beta 50.4794 32.11354 0.904656 1.386477 13.57246 13.75161 Iteration 18 Estimate of theta 1.1374 Iteration 18 GLS estimate of beta 50.4794 32.11354 0.904656 1.386477 13.57246 13.75161 Iteration 19 Estimate of theta 1.1374 Iteration 19 GLS estimate of beta 50.4794 32.11354 0.904656 1.386477 13.57246 13.75161 Iteration 20 Estimate of theta 1.1374 Iteration 20 GLS estimate of beta 50.4794 32.11354 0.904656 1.386477 13.57246 13.75161 Final estimate of sigma 0.027036 Final estimate of theta 1.137408 Formula: ywt ~ weightfunc(x, W0, W1, beta0, beta1, tau0, tau1, v, wt) Parameters: Estimate Std. Error t value Pr(>|t|) W0 50.47940 1.46998 34.340 < 2e-16 *** W1 32.11354 1.93274 16.616 1.63e-11 *** beta0 0.90466 0.02385 37.927 < 2e-16 *** beta1 1.38648 0.35235 3.935 0.00118 ** tau0 13.57246 0.81779 16.596 1.66e-11 *** tau1 13.75161 1.95457 7.036 2.81e-06 *** --- Signif. codes: 0 ‘***’ 0.001 ‘**’ 0.01 ‘*’ 0.05 ‘.’ 0.1 ‘ ’ 1 Residual standard error: 0.02704 on 16 degrees of freedom Number of iterations to convergence: 5 Achieved convergence tolerance: 2.457e-06